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FreeZone 4.5 Liter Benchtop Freeze Dry Systems

Free Flask The FreeZone 4.5 Liter Benchtop Freeze Dry System is a compact laboratory lyophilizer with ice holding capacity for light to moderate sample loads. It has a permanently-installed 10-port drying chamber and a compact benchtop design. A vacuum pump and sample containers, such as flasks, are the only additional components necessary for a complete system. NOTE: These freeze dryers are not recommended for use with samples containing acetonitrile. If your samples contain acetonitrile, please see FreeZone Freeze Dry Systems with cascade refrigeration.

FreeZone 4.5 Liter Benchtop Freeze Dry Systems

Catalog # Summary
7750020 Domestic Electrical
7750030 International Electrical
7750040 Domestic Electrical

FreeZone 4.5 Liter Benchtop Freeze Dry System with Teflon-Coated Collector

Catalog # Summary
7750021 Domestic Electrical
7750031 International Electrical
7750041 Domestic Electrical
A Guide to Freeze Drying for the Laboratory Industry service publication which provides background information on the principles of freeze drying.
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Recommended by Labconco!
FreeZone 4.5 Liter Freeze Dry Systems Manual For catalog numbers: 7750020, 7750021, 7750030, 7750031, 7750040, 7750041, 7751020, 7751021, 7751030, 7751031, 7751040, 7751041
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Chemical Resistance of Freeze Dryer Components Provides information on the level of resistance Freeze Dryer components have toward a number of commonly used chemicals.
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Freeze Dry Vacuum System Troubleshooting Provides instructions and illustrations to help solve vacuum leaks.
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FreeZone Freeze Dry Systems: Quick Guide to Installation
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Lexsol 542 MSDS Material safety data sheet for heat transfer solution used in FreeZone Stoppering Tray Dryers and FreeZone Triad Freeze Dry Systems.
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Methodologies using the Freeze Dryer Approximate Freeze Drying Times, Procedure for Freeze Drying Fish Samples for Volatile Substances Using a 4.5 Liter Freeze Dry System, Extraction and Analytical Method for "Microcystin LR" in Cyanobacteria Samples, General Freeze Dry Application for Snake Venom and Other Small Volume Samples of 0.4 ml or Less, Freeze Drying Fungi, General Freeze Dry Application for Monitoring Soil Samples, Freeze Dry Applications for Monitoring Anti-Cancer Drugs and Freeze Drying Mango Powder.
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Concentration of Solutes: Options for the Removal of Solvents from Samples Briefly discusses the various options for removing solvents including evaporation, vacuum concentration, lyophilization, reverse extraction, dialysis and precipitation.
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With so many freeze dryers, how do you choose? Here are some pointers.
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How to Build a Freeze Dry System
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Application of Glutathione in Protecting Freeze Dried Biomolecules Article describes how glutathione prevents oxidation until a freeze dried sample is reconstituted.
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Installation Qualification/Operation Qualification for FreeZone Freeze Dry Systems For validation of predetermined FreeZone Freeze Dry Systems specifications. Provides a checklist of installation and operation qualifications to complete when beginning operation on new or used FreeZone Freeze Dry Systems manufactured in 2004 or later. These systems have blue control panel labels and stainless steel fronts. Part number is 1059500 Rev_.
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Compliance

• UL Standard 61010A-1 (60 Hz models)
• CAN/CSA C22.2 No. 1010.1 (60 Hz models)
CE Conformity marking (220/240 volts, 50 Hz models)

Features

• Upright stainless steel collector coil capable of removing over 2 liters of water in 24 hours and holding 4.5 liters of ice before defrosting
• 1/3 hp CFC-free refrigeration system to cool collector to -50° C (-58° F)
• Permanently-installed 10-port stainless steel drying chamber with 3/4" thick acrylic lid with neoprene gasket
• Compact benchtop design with a small footprint
• Corrosion-resistant glacier white epoxy-coated steel and brushed stainless steel exterior with blue accents
• LCD that displays system operating parameters, set up parameters and alarm messages. It may be user-configured to display vacuum in mBar, Pa or Torr and temperature in °F or °C. It also displays total number of hours of refrigeration operation and since the refrigeration was serviced and the total number of hours of vacuum pump operation and since the vacuum pump was serviced
• Red alarm light that flashes and beeper that sounds to indicate that an abnormal system event has occurred, including: power failure, improper line voltage supply, collector temperature rise above -40° C, service vacuum pump (after 1000 hours of vacuum use), and moisture in collector. Pressing the Menu Switch displays the alarm message on the LCD
• LED vacuum and temperature "waves" for at-a-glance display of relative system vacuum and collector temperature
• Patented moisture sensor that prevents refrigeration or vacuum start up when moisture is detected in the collector chamber area
• Vacuum control valve that maintains setpoint vacuum level
• Vacuum break valve that bleeds air into the system when power to the freeze dryer or vacuum pump is shut off
• Rear-mounted RS-232 port to transmit data to a user-supplied computer
• Automatic start-up switch for collector cool down and vacuum pull down with manual override switches
• Side-mounted, retractable, 9" collector drain line
• Side-mounted power switch and rear-mounted electrical receptacle (for vacuum pump connection)
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and two clamps
ETL Listing (60 Hz models)

Options

• Teflon-coated collector chamber and coil for processes involving corrosive compounds
• Domestic or international electrical configuration

Required Accessories

Rotary Vane Direct Drive Vacuum Pump with a minimum displacement of 86 liters/minute, 0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum hose
Freeze dry glassware

Optional Accessories

• Support shelves that mount on either side of the freeze dryer to support glassware attached to the drying chamber
• With Attachment Port Lid 7762800 attached (sold separately), Manifold 7522400, Heated Drying Chamber 7521000, 7521001 or Clear Drying Chamber 7867000 may be mounted atop the freeze dryer
Laboratory Carts & Benches
Traps and Other Vacuum Pump Accessories